With the deepening of the new round of scientific and technological revolution and industrial transformation, as well as the advancement of the “dual carbon” strategy, higher requirements have been put forward for the innovative, practical, and interdisciplinary literacy of engineering and technical talents. After the launch of Emerging Engineering Education, experimental teaching reform has become the core link in the transformation of engineering education paradigm. As a municipal key university specializing in engineering, the University of Shanghai for Science and Technology (USST) has a development orientation in line with the requirements of Emerging Engineering Education and has carried out comprehensive teaching reforms. The Institute of Energy Materials Science has also introduced cutting-edge electrochemical projects into undergraduate experiments, but a systematic new system of electrochemical experiment teaching has not yet been formed. Taking the electrochemical experiment teaching of USST as the research object, this paper analyzes the common bottlenecks and personalized needs of experimental teaching under the background of Emerging Engineering Education, and explores the construction of a comprehensive reform plan of “value guidance, ability orientation, digital empowerment, and industry-education collaboration.” Centered on the systematic reconstruction of teaching content, the reform links five aspects: teaching mode, digital platform, diversified evaluation, and industry-education collaboration mechanism. It aims to promote the transformation of experimental teaching from a verification link to a core position for ability training, cultivate outstanding engineering and technological talents adapting to industrial needs, and provide a referable demonstration paradigm for practical teaching reform in similar local engineering universities.